Curriculum/Pensum KJM 5250 / KJM 9250

Recommended reading: Timothy, D. W. Claridge: High-Resolution NMR Techniques in Organic Chemistry, Third Edition Elsevier. ISBN: 978-0-08-099986-9. Obtain it from the University Book Store or for instance at:

https://www.amazon.co.uk/High-Resolution-NMR-Techniques-Organic-Chemistry/dp/0080999867/ref=sr_1_55?s=books&ie=UTF8&qid=1513759786&sr=1-55&keywords=nmr+spectroscopy

Recommended reading: Timothy, D. W. Claridge: High-Resolution NMR Techniques in Organic Chemistry, Third Edition Elsevier. ISBN: 978-0-08-099986-9. Obtain it from the University Book Store or for instance at:

https://www.amazon.co.uk/High-Resolution-NMR-Techniques-Organic-Chemistry/dp/0080999867/ref=sr_1_55?s=books&ie=UTF8&qid=1513759786&sr=1-55&keywords=nmr+spectroscopy

Start with chapter 13.  Structure Elucidation and Spectrum Assignment. Pages 500-525.

Continue with chapters 1, 2 and 3 pages 1-130.

Chapter 4. Pages 133 - 165.  Some pages will be defined as cursory later.

Chapter 5. Pages 172 – 188.  Other topics will be touched briefly.

Chapter 6. .Pages 203 – 235.  Some pages will be defined as cursory later.

Chapter 7.  Pages 243 – 291.  Some pages will be defined as cursory later.

Chapter 8. Cursory curriculum.  

Chapter 9 Correlation Through Space: The Nuclear Overhauser Effect. Pages 315 – 359 and 367-368 (section 9.10).

Chapter 12. Cursory curriculum.  Topics will be touched upon at the spectrometers. (12.2, 12.3, 12.4 and 12.5)

Chapters 10 and 11. Diffusion NMR spectroscopy (pages 381-418) and Protein-Ligand screening by NMR (pages 421 – 454) are not included in the curriculum.

If you find the book difficult to read you can alternatively start reading the book written by Horst Friebolin: "Basic One-and Two-dimensional NMR Spectroscopy", third revised edition, ISBN: 3-527-29513-5.

The web resource:

http://www.magritek.com/products/terranova/videos/

is a good place to learn nmr.  These videos will be used in the lectures.  Videos 8-10 is not curriculum in KJM 5250 but constitute the extra curriculum (introductory MRI) that is contained in the cloned PhD course KJM 9250.

The web pages:

http://www.cis.rit.edu/htbooks/nmr/inside.htm

is quite helpful and you can learn a lot yourself watching them again and again.

The most important part of the course consists of the combined colloquium experiments which will be selected from the following two web pages:

https://www.mn.uio.no/kjemi/english/research/about/infrastructure/nmr/manuals/KJM5250endingspring2018

http://www.mn.uio.no/kjemi/english/research/about/infrastructure/nmr/manuals/KJM9250fromspring2018

 

Publisert 10. jan. 2018 12:25 - Sist endret 13. feb. 2018 13:36