Curriculum/Pensum KJM 5250 / KJM 9250
Recommended reading: Timothy, D. W. Claridge: High-Resolution NMR Techniques in Organic Chemistry, Third Edition Elsevier. ISBN: 978-0-08-099986-9. Obtain it from the University Book Store or for instance at:
Recommended reading: Timothy, D. W. Claridge: High-Resolution NMR Techniques in Organic Chemistry, Third Edition Elsevier. ISBN: 978-0-08-099986-9. Obtain it from the University Book Store or for instance at:
Start with chapter 13. Structure Elucidation and Spectrum Assignment. Pages 500-525.
Continue with chapters 1, 2 and 3 pages 1-130.
Chapter 4. Pages 133 - 165. Some pages will be defined as cursory later.
Chapter 5. Pages 172 – 188. Other topics will be touched briefly.
Chapter 6. .Pages 203 – 235. Some pages will be defined as cursory later.
Chapter 7. Pages 243 – 291. Some pages will be defined as cursory later.
Chapter 8. Cursory curriculum.
Chapter 9 Correlation Through Space: The Nuclear Overhauser Effect. Pages 315 – 359 and 367-368 (section 9.10).
Chapter 12. Cursory curriculum. Topics will be touched upon at the spectrometers. (12.2, 12.3, 12.4 and 12.5)
Chapters 10 and 11. Diffusion NMR spectroscopy (pages 381-418) and Protein-Ligand screening by NMR (pages 421 – 454) are not included in the curriculum.
If you find the book difficult to read you can alternatively start reading the book written by Horst Friebolin: "Basic One-and Two-dimensional NMR Spectroscopy", third revised edition, ISBN: 3-527-29513-5.
The web resource:
http://www.magritek.com/products/terranova/videos/
is a good place to learn nmr. These videos will be used in the lectures. Videos 8-10 is not curriculum in KJM 5250 but constitute the extra curriculum (introductory MRI) that is contained in the cloned PhD course KJM 9250.
The web pages:
http://www.cis.rit.edu/htbooks/nmr/inside.htm
is quite helpful and you can learn a lot yourself watching them again and again.
The most important part of the course consists of the combined colloquium/laboratory experiments which will be selected from the following three web pages: